PetroChina Company Limited
Low viscosity poly-a-olefin lubricating oil and synthesis method thereof
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Abstract:
The present invention provides a low viscosity poly-.alpha.-olefin lubricating oil and a synthesis method thereof. The method comprises: (1) the .alpha.-olefin raw material is subjected to dehydration treatment so that the water content in the raw material is .ltoreq.10 ppm; (2) a reaction of the dehydration treated .alpha.-olefin raw material is carried out in the presence of a complex catalyst and gaseous BF.sub.3 to obtain a reaction product, wherein the pressure of the gaseous BF.sub.3 is 0.01 to 1 MPa; (3) the reaction product obtained in step (2) is sequentially subjected to flash distillation, gas stripping, centrifugation, and washing treatment to obtain an intermediate product; (4) the intermediate product obtained in step (3) is subjected to distillation under reduced pressure to separate the unreacted .alpha.-olefin raw material and .alpha.-olefin dimers, and the remaining heavy fractions are subjected to hydrogenation saturation treatment followed by fractionation and cutting-off.
Utility
24 Oct 2019
7 Jun 2022